TA Instruments

AR1696-0001f

04/09/2012 14:50:38

Sample name	ASW 10 mm from base, 60 mm to top, disk 24
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1696
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 14:50:38

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-13.03	5.455	-2.388	1.0000	22.4	51.25	1.8410	10000	0.01258	1.723	2.3013	230.13	3.384E-3	0.0	1.0	61.000	-39.961	4.364
0.7781	12.54	0.06207	2.0000	22.4	68.61	13.4793	10000	0.01684	0.4366	16.849	1684.9	3.383E-3	0.0	1.0	62.000	2.3872	10.03
1.573	19.46	0.08084	2.9960	22.4	54.56	27.1422	10000	0.01339	0.1441	33.928	3392.8	3.383E-3	0.0	1.0	62.996	4.8263	15.57
2.078	23.12	0.08988	4.0000	22.4	57.87	41.0892	10000	0.01420	0.1083	51.362	5136.2	3.384E-3	0.1	1.1	64.000	6.3753	18.50
3.358	30.91	0.1087	5.0000	22.4	60.35	67.8090	10000	0.01481	0.06317	84.761	8476.1	3.384E-3	0.1	1.1	65.000	10.304	24.73
5.282	39.54	0.1336	5.9960	22.4	61.17	107.0730	10000	0.01501	0.03914	133.84	13384	3.384E-3	0.1	1.1	65.996	16.206	31.63
5.989	42.58	0.1406	6.9960	22.4	51.25	126.5340	10000	0.01258	0.02827	158.17	15817	3.383E-3	0.1	1.1	66.996	18.373	34.07
7.598	49.17	0.1545	8.0000	22.4	52.91	165.7250	10000	0.01299	0.02188	207.16	20716	3.383E-3	0.1	1.1	68.000	23.311	39.34
10.35	57.57	0.1797	9.0000	22.4	56.21	223.4310	10000	0.01380	0.01696	279.29	27929	3.384E-3	0.2	1.2	69.000	31.744	46.06
12.10	63.72	0.1899	10.000	22.4	37.20	275.2040	10000	9.130E-3	9.161E-3	344.01	34401	3.384E-3	0.2	1.2	70.000	37.134	50.98
14.20	69.68	0.2038	10.996	22.4	50.43	326.2660	10000	0.01238	0.01039	407.83	40783	3.383E-3	0.2	1.2	70.996	43.572	55.74
16.14	75.14	0.2147	12.000	22.4	63.65	377.4580	10000	0.01562	0.01127	471.82	47182	3.383E-3	0.2	1.2	72.000	49.506	60.12
18.15	80.54	0.2254	12.992	22.4	39.68	435.7590	10000	9.739E-3	6.118E-3	544.70	54470	3.384E-3	0.2	1.2	72.992	55.680	64.43
20.31	86.45	0.2349	13.996	22.4	30.59	498.7630	10000	7.507E-3	4.092E-3	623.45	62345	3.384E-3	0.2	1.2	73.996	62.312	69.16
23.50	94.62	0.2484	14.996	22.4	39.68	594.6960	10000	9.739E-3	4.432E-3	743.37	74337	3.384E-3	0.2	1.2	74.996	72.095	75.69
25.55	99.93	0.2556	15.996	22.4	35.55	664.4040	10000	8.724E-3	3.560E-3	830.51	83051	3.383E-3	0.3	1.3	75.996	78.372	79.94
27.87	105.7	0.2637	16.996	22.4	46.29	740.7580	10000	0.01136	4.145E-3	925.95	92595	3.383E-3	0.3	1.3	76.996	85.504	84.54
31.32	113.7	0.2754	18.004	22.4	31.41	855.1610	10000	7.710E-3	2.428E-3	1069.0	1.0690E5	3.384E-3	0.3	1.3	78.004	96.085	90.99
33.45	118.8	0.2815	19.000	22.4	34.72	931.3280	10000	8.521E-3	2.460E-3	1164.2	1.1642E5	3.384E-3	0.3	1.3	79.000	102.62	95.05
35.92	124.3	0.2891	20.000	22.4	28.11	1020.8000	10000	6.898E-3	1.820E-3	1276.0	1.2760E5	3.384E-3	0.3	1.3	80.000	110.21	99.41
39.87	132.3	0.3014	21.000	22.4	35.55	1155.4200	10000	8.724E-3	2.031E-3	1444.3	1.4443E5	3.384E-3	0.4	1.4	81.000	122.32	105.8
42.40	137.4	0.3086	22.000	22.4	17.36	1243.4600	10000	4.261E-3	9.198E-4	1554.3	1.5543E5	3.384E-3	0.4	1.4	82.000	130.08	109.9
44.96	142.8	0.3148	22.996	22.4	9.920	1343.6300	10000	2.435E-3	4.865E-4	1679.5	1.6795E5	3.384E-3	0.4	1.4	82.996	137.92	114.2
49.12	150.8	0.3257	24.000	22.4	14.05	1495.6500	10000	3.449E-3	6.179E-4	1869.6	1.8696E5	3.384E-3	0.4	1.4	84.000	150.70	120.6
51.87	155.9	0.3327	24.996	22.4	-14.88	1598.7300	10000	-3.652E-3	-6.120E-4	1998.4	1.9984E5	3.384E-3	0.4	1.4	84.996	159.13	124.7
54.19	161.3	0.3359	25.996	22.4	6.613	1711.0300	10000	1.623E-3	2.541E-4	2138.8	2.1388E5	3.384E-3	0.4	1.4	85.996	166.25	129.1
59.08	169.3	0.3489	26.996	22.4	-10.75	1882.4000	10000	-2.638E-3	-3.748E-4	2353.0	2.3530E5	3.384E-3	0.4	1.4	86.996	181.26	135.5
62.49	174.4	0.3582	27.996	22.4	-4.133	1995.8000	10000	-1.014E-3	-1.358E-4	2494.8	2.4948E5	3.384E-3	0.5	1.5	87.996	191.70	139.6
64.77	179.6	0.3607	29.000	22.4	-3.307	2116.1299	10000	-8.116E-4	-1.026E-4	2645.2	2.6452E5	3.384E-3	0.5	1.5	89.000	198.71	143.6
69.11	187.6	0.3685	29.996	22.4	-4.133	2306.1499	10000	-1.014E-3	-1.175E-4	2882.7	2.8827E5	3.383E-3	0.5	1.5	89.996	212.04	150.0
72.49	192.7	0.3762	30.996	22.4	-16.53	2432.9199	10000	-4.058E-3	-4.453E-4	3041.2	3.0412E5	3.384E-3	0.5	1.5	90.996	222.39	154.2
75.59	197.8	0.3821	31.996	22.4	-10.75	2565.6101	10000	-2.638E-3	-2.746E-4	3207.0	3.2070E5	3.384E-3	0.5	1.5	91.996	231.90	158.3
80.16	205.8	0.3895	32.996	22.4	-29.76	2774.7900	10000	-7.304E-3	-7.025E-4	3468.5	3.4685E5	3.384E-3	0.5	1.5	92.996	245.93	164.7
82.94	211.0	0.3931	34.000	22.4	-24.80	2912.4800	10000	-6.087E-3	-5.572E-4	3640.6	3.6406E5	3.384E-3	0.6	1.6	94.000	254.45	168.8
88.94	218.6	0.4069	35.000	22.4	-48.77	3129.2000	10000	-0.01197	-1.021E-3	3911.5	3.9115E5	3.383E-3	0.6	1.6	95.000	272.86	174.9
92.20	223.9	0.4118	35.996	22.4	-38.03	3280.5000	10000	-9.333E-3	-7.586E-4	4100.6	4.1006E5	3.383E-3	0.6	1.6	95.996	282.86	179.1
95.83	229.1	0.4184	36.996	22.4	-38.85	3431.3301	10000	-9.536E-3	-7.404E-4	4289.2	4.2892E5	3.384E-3	0.6	1.6	96.996	294.02	183.3
100.0	236.6	0.4228	37.996	22.4	-42.99	3657.9500	10000	-0.01055	-7.677E-4	4572.4	4.5724E5	3.384E-3	0.6	1.6	97.996	306.92	189.3
104.0	241.8	0.4301	38.996	22.4	-35.55	3822.1001	10000	-8.724E-3	-6.078E-4	4777.6	4.7776E5	3.383E-3	0.6	1.6	98.996	319.13	193.5
108.7	249.6	0.4354	40.000	22.4	-53.73	4068.3601	10000	-0.01319	-8.626E-4	5085.5	5.0855E5	3.383E-3	0.7	1.7	100.000	333.42	199.7
111.9	254.6	0.4394	40.996	22.4	-57.87	4232.5498	10000	-0.01420	-8.926E-4	5290.7	5.2907E5	3.383E-3	0.7	1.7	100.996	343.22	203.7
117.4	259.8	0.4517	41.996	22.4	-86.80	4410.8198	10000	-0.02130	-1.286E-3	5513.5	5.5135E5	3.384E-3	0.7	1.7	101.996	360.10	207.9
121.9	267.6	0.4555	42.996	22.4	-75.23	4674.3101	10000	-0.01846	-1.050E-3	5842.9	5.8429E5	3.384E-3	0.7	1.7	102.996	373.94	214.1
125.0	272.7	0.4583	43.996	22.4	-62.00	4851.2300	10000	-0.01522	-8.339E-4	6064.0	6.0640E5	3.384E-3	0.7	1.7	103.996	383.36	218.1
131.9	280.3	0.4705	44.996	22.4	-86.80	5133.7402	10000	-0.02130	-1.104E-3	6417.2	6.4172E5	3.384E-3	0.7	1.7	104.996	404.62	224.3
133.9	285.5	0.4689	45.996	22.4	-76.88	5318.0200	10000	-0.01887	-9.431E-4	6647.5	6.6475E5	3.383E-3	0.8	1.8	105.996	410.72	228.4
141.0	293.1	0.4811	46.996	22.4	-99.20	5601.8999	10000	-0.02435	-1.155E-3	7002.4	7.0024E5	3.384E-3	0.8	1.8	106.996	432.58	234.5
144.8	298.1	0.4855	47.996	22.4	-90.93	5797.5801	10000	-0.02232	-1.023E-3	7247.0	7.2470E5	3.384E-3	0.8	1.8	107.996	444.11	238.5
147.0	303.3	0.4847	48.996	22.4	-79.36	5999.4702	10000	-0.01948	-8.625E-4	7499.3	7.4993E5	3.383E-3	0.8	1.8	108.996	451.05	242.7
152.0	311.0	0.4888	49.996	22.4	-76.88	6302.2202	10000	-0.01887	-7.951E-4	7877.8	7.8778E5	3.383E-3	0.8	1.8	109.996	466.28	248.8
156.8	316.0	0.4962	50.996	22.4	-78.53	6510.3198	10000	-0.01927	-7.864E-4	8137.9	8.1379E5	3.383E-3	0.8	1.8	110.996	481.04	252.8
164.2	323.8	0.5072	51.996	22.4	-100.0	6833.6299	10000	-0.02455	-9.541E-4	8542.0	8.5420E5	3.384E-3	0.9	1.9	111.996	503.79	259.0
165.2	328.9	0.5023	52.996	22.4	-87.62	7046.4199	10000	-0.02151	-8.102E-4	8808.0	8.8080E5	3.384E-3	0.9	1.9	112.996	506.81	263.1
171.8	336.4	0.5107	53.996	22.4	-109.9	7374.3101	10000	-0.02698	-9.715E-4	9217.9	9.2179E5	3.383E-3	0.9	1.9	113.996	527.09	269.1
176.9	341.6	0.5178	54.996	22.4	-100.9	7601.2700	10000	-0.02475	-8.643E-4	9501.6	9.5016E5	3.383E-3	0.9	1.9	114.996	542.68	273.3
178.8	346.7	0.5158	55.996	22.4	-85.15	7828.2598	10000	-0.02090	-7.083E-4	9785.3	9.7853E5	3.384E-3	0.9	1.9	115.996	548.61	277.4
187.2	354.2	0.5286	56.996	22.4	-87.62	8171.0000	10000	-0.02151	-6.984E-4	10214	1.0214E6	3.384E-3	0.9	1.9	116.996	574.37	283.4
189.7	359.4	0.5280	57.996	22.4	-81.84	8408.3701	10000	-0.02009	-6.337E-4	10510	1.0510E6	3.383E-3	1.0	2.0	117.996	582.13	287.5
195.6	367.0	0.5329	58.996	22.4	-119.0	8767.7002	10000	-0.02922	-8.838E-4	10960	1.0960E6	3.383E-3	1.0	2.0	118.996	600.02	293.6
203.4	372.0	0.5468	59.996	22.4	-138.9	9007.2900	10000	-0.03409	-1.004E-3	11259	1.1259E6	3.384E-3	1.0	2.0	119.996	624.07	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

204.1	375.0	0.5441	1.0120	22.4	-135.6	301.2830	10000	-0.03327	-9.640E-4	376.60	37660	3.384E-3	0.0	2.0	122.012	626.03	300.0
207.0	375.0	0.5520	1.9960	22.4	-149.6	552.5120	10000	-0.03672	-1.064E-3	690.64	69064	3.384E-3	0.0	2.0	122.996	635.03	300.0
205.1	375.0	0.5470	3.0120	22.4	-136.4	803.9000	10000	-0.03348	-9.698E-4	1004.9	1.0049E5	3.384E-3	0.1	2.1	124.012	629.36	300.0
204.7	375.0	0.5458	4.0160	22.4	-129.8	1183.2200	10000	-0.03185	-9.229E-4	1479.0	1.4790E5	3.383E-3	0.1	2.1	125.016	627.95	300.0
207.3	375.0	0.5527	5.0120	22.4	-130.6	1432.2000	10000	-0.03206	-9.288E-4	1790.3	1.7903E5	3.384E-3	0.1	2.1	126.012	635.87	300.0
206.8	375.0	0.5514	6.0000	22.4	-126.5	1809.7600	10000	-0.03104	-8.994E-4	2262.2	2.2622E5	3.383E-3	0.1	2.1	127.000	634.41	300.0
205.0	375.0	0.5467	7.0120	22.4	-111.6	2082.3301	10000	-0.02739	-7.936E-4	2602.9	2.6029E5	3.383E-3	0.1	2.1	128.012	628.94	300.0
204.9	375.0	0.5463	8.0120	22.4	-107.5	2311.8301	10000	-0.02638	-7.642E-4	2889.8	2.8898E5	3.384E-3	0.1	2.2	129.012	628.51	300.0
204.7	375.0	0.5460	9.0120	22.4	-132.3	2688.8999	10000	-0.03246	-9.405E-4	3361.1	3.3611E5	3.384E-3	0.2	2.2	130.012	628.14	300.0
205.8	375.0	0.5487	10.012	22.4	-120.7	2941.4900	10000	-0.02962	-8.583E-4	3676.9	3.6769E5	3.383E-3	0.2	2.2	131.012	631.26	300.0
208.9	375.0	0.5570	11.016	22.4	-153.8	3317.2100	10000	-0.03774	-1.093E-3	4146.5	4.1465E5	3.383E-3	0.2	2.2	132.016	640.76	300.0
203.5	375.0	0.5428	12.016	22.4	-127.3	3572.6699	10000	-0.03125	-9.053E-4	4465.8	4.4658E5	3.384E-3	0.2	2.2	133.016	624.43	300.0
207.3	375.0	0.5528	13.012	22.4	-134.7	3819.7800	10000	-0.03307	-9.582E-4	4774.7	4.7747E5	3.384E-3	0.2	2.2	134.012	635.99	300.0
206.9	375.0	0.5517	14.016	22.4	-129.0	4196.9399	10000	-0.03165	-9.170E-4	5246.2	5.2462E5	3.383E-3	0.2	2.3	135.016	634.74	300.0
206.1	375.0	0.5496	15.012	22.4	-144.7	4448.0400	10000	-0.03551	-1.029E-3	5560.1	5.5601E5	3.384E-3	0.3	2.3	136.012	632.34	300.0
206.5	375.0	0.5507	16.012	22.4	-100.9	4827.7798	10000	-0.02475	-7.171E-4	6034.7	6.0347E5	3.384E-3	0.3	2.3	137.012	633.63	300.0
204.9	375.0	0.5464	17.016	22.4	-125.7	5076.4800	10000	-0.03084	-8.935E-4	6345.6	6.3456E5	3.383E-3	0.3	2.3	138.016	628.62	300.0
205.1	375.0	0.5469	18.012	22.4	-98.37	5328.8501	10000	-0.02414	-6.996E-4	6661.1	6.6611E5	3.383E-3	0.3	2.3	139.012	629.13	300.0
206.8	375.0	0.5514	18.996	22.4	-153.8	5704.8301	10000	-0.03774	-1.093E-3	7131.0	7.1310E5	3.384E-3	0.3	2.3	139.996	634.41	300.0
207.7	375.0	0.5538	20.012	22.4	-118.2	5956.9902	10000	-0.02901	-8.406E-4	7446.2	7.4462E5	3.384E-3	0.3	2.4	141.012	637.12	300.0
205.3	375.0	0.5475	21.012	22.4	-115.7	6207.4600	10000	-0.02840	-8.229E-4	7759.3	7.7593E5	3.384E-3	0.4	2.4	142.012	629.94	300.0
207.3	375.0	0.5528	22.016	22.4	-161.2	6584.5000	10000	-0.03956	-1.146E-3	8230.6	8.2306E5	3.383E-3	0.4	2.4	143.016	636.04	300.0
206.4	375.0	0.5504	23.016	22.4	-123.2	6836.9399	10000	-0.03023	-8.758E-4	8546.2	8.5462E5	3.383E-3	0.4	2.4	144.016	633.20	300.0
205.2	375.0	0.5473	24.012	22.4	-105.8	7212.7998	10000	-0.02597	-7.524E-4	9016.0	9.0160E5	3.384E-3	0.4	2.4	145.012	629.63	300.0
206.0	375.0	0.5492	25.016	22.4	-99.20	7470.1802	10000	-0.02435	-7.054E-4	9337.7	9.3377E5	3.384E-3	0.4	2.4	146.016	631.89	300.0
208.1	375.0	0.5550	26.016	22.4	-146.3	7716.9199	10000	-0.03591	-1.040E-3	9646.2	9.6462E5	3.384E-3	0.4	2.5	147.016	638.50	300.0
208.1	375.0	0.5548	27.016	22.4	-144.7	8092.4102	10000	-0.03551	-1.029E-3	10116	1.0116E6	3.383E-3	0.5	2.5	148.016	638.32	300.0
206.3	375.0	0.5501	28.012	22.4	-129.8	8345.8896	10000	-0.03185	-9.229E-4	10432	1.0432E6	3.384E-3	0.5	2.5	149.012	632.92	300.0
208.3	375.0	0.5555	29.016	22.4	-138.9	8723.5498	10000	-0.03409	-9.877E-4	10904	1.0904E6	3.384E-3	0.5	2.5	150.016	639.03	300.0
206.6	375.0	0.5510	30.012	22.4	-81.01	8976.4697	10000	-0.01988	-5.761E-4	11221	1.1221E6	3.384E-3	0.5	2.5	151.012	633.92	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

201.3	370.0	0.5439	1.0120	22.4	-76.05	318.7110	10000	-0.01867	-5.555E-4	398.39	39839	3.384E-3	0.0	2.5	152.012	617.44	296.0
199.8	365.0	0.5473	2.0120	22.4	-119.0	555.2750	10000	-0.02922	-8.935E-4	694.09	69409	3.384E-3	0.0	2.6	153.012	612.84	292.0
193.6	359.9	0.5378	3.0120	22.4	-155.4	793.2680	10000	-0.03814	-1.200E-3	991.59	99159	3.383E-3	0.1	2.6	154.012	593.85	288.0
187.8	352.3	0.5330	4.0120	22.4	-115.7	1144.0100	10000	-0.02840	-9.327E-4	1430.0	1.4300E5	3.384E-3	0.1	2.6	155.012	576.07	281.8
183.8	347.3	0.5294	5.0160	22.4	-100.0	1369.2600	10000	-0.02455	-8.294E-4	1711.6	1.7116E5	3.384E-3	0.1	2.6	156.016	563.99	277.8
175.4	339.7	0.5165	6.0120	22.4	-78.53	1707.4200	10000	-0.01927	-6.807E-4	2134.3	2.1343E5	3.383E-3	0.1	2.6	157.012	538.26	271.7
173.7	334.5	0.5193	7.0120	22.4	-108.3	1932.9301	10000	-0.02658	-9.679E-4	2416.2	2.4162E5	3.384E-3	0.1	2.6	158.012	532.86	267.6
163.6	326.9	0.5005	8.0120	22.4	-78.53	2252.2000	10000	-0.01927	-7.347E-4	2815.3	2.8153E5	3.384E-3	0.1	2.7	159.012	502.04	261.6
160.4	321.9	0.4982	9.0160	22.4	-102.5	2464.9500	10000	-0.02516	-9.894E-4	3081.2	3.0812E5	3.384E-3	0.2	2.7	160.016	491.99	257.5
158.3	316.7	0.4998	10.012	22.4	-86.80	2677.6299	10000	-0.02130	-8.653E-4	3347.0	3.3470E5	3.384E-3	0.2	2.7	161.012	485.66	253.4
150.9	309.0	0.4884	11.012	22.4	-70.27	2984.5000	10000	-0.01725	-7.357E-4	3730.6	3.7306E5	3.384E-3	0.2	2.7	162.012	463.06	247.2
149.0	304.0	0.4903	12.008	22.4	-85.15	3184.7900	10000	-0.02090	-9.214E-4	3981.0	3.9810E5	3.384E-3	0.2	2.7	163.008	457.26	243.2
140.7	296.3	0.4748	13.020	22.4	-71.92	3485.1699	10000	-0.01765	-8.194E-4	4356.5	4.3565E5	3.384E-3	0.2	2.7	164.020	431.57	237.0
140.7	291.1	0.4833	14.012	22.4	-67.79	3679.0300	10000	-0.01664	-8.002E-4	4598.8	4.5988E5	3.384E-3	0.2	2.8	165.012	431.59	232.8
133.9	283.5	0.4722	15.020	22.4	-68.61	3960.6399	10000	-0.01684	-8.538E-4	4950.8	4.9508E5	3.384E-3	0.3	2.8	166.020	410.70	226.8
128.6	278.3	0.4620	16.020	22.4	-45.47	4148.3999	10000	-0.01116	-5.869E-4	5185.5	5.1855E5	3.383E-3	0.3	2.8	167.020	394.47	222.7
123.2	273.1	0.4512	17.016	22.4	-36.37	4329.7500	10000	-8.927E-3	-4.876E-4	5412.2	5.4122E5	3.383E-3	0.3	2.8	168.016	378.11	218.5
122.3	265.6	0.4604	18.012	22.4	-57.87	4592.4702	10000	-0.01420	-8.204E-4	5740.6	5.7406E5	3.383E-3	0.3	2.8	169.012	375.17	212.5
116.4	260.4	0.4468	19.012	22.4	-42.16	4767.4302	10000	-0.01035	-6.216E-4	5959.3	5.9593E5	3.383E-3	0.3	2.8	170.012	356.97	208.3
111.4	252.6	0.4412	20.012	22.4	-50.43	5029.9399	10000	-0.01238	-7.902E-4	6287.4	6.2874E5	3.384E-3	0.3	2.9	171.012	341.91	202.1
108.3	247.6	0.4374	21.000	22.4	-45.47	5186.5200	10000	-0.01116	-7.417E-4	6483.2	6.4832E5	3.384E-3	0.4	2.9	172.000	332.23	198.1
105.2	242.4	0.4337	22.012	22.4	-28.11	5348.9600	10000	-6.898E-3	-4.782E-4	6686.2	6.6862E5	3.384E-3	0.4	2.9	173.012	322.63	194.0
99.31	234.6	0.4234	23.008	22.4	-36.37	5592.7202	10000	-8.927E-3	-6.612E-4	6990.9	6.9909E5	3.383E-3	0.4	2.9	174.008	304.68	187.6
95.45	229.4	0.4160	24.012	22.4	-23.97	5742.8701	10000	-5.884E-3	-4.554E-4	7178.6	7.1786E5	3.384E-3	0.4	2.9	175.012	292.85	183.5
89.54	221.7	0.4038	25.020	22.4	-13.23	5968.0200	10000	-3.246E-3	-2.690E-4	7460.0	7.4600E5	3.384E-3	0.4	2.9	176.020	274.71	177.4
87.85	216.4	0.4059	26.012	22.4	-9.920	6117.7402	10000	-2.435E-3	-2.118E-4	7647.2	7.6472E5	3.383E-3	0.4	3.0	177.012	269.53	173.1
82.84	211.3	0.3920	27.016	22.4	-9.093	6256.1001	10000	-2.232E-3	-2.036E-4	7820.1	7.8201E5	3.383E-3	0.5	3.0	178.016	254.15	169.1
78.30	203.7	0.3844	28.012	22.4	-6.613	6461.3799	10000	-1.623E-3	-1.594E-4	8076.7	8.0767E5	3.384E-3	0.5	3.0	179.012	240.22	162.9
75.03	198.4	0.3782	29.012	22.4	-0.8267	6599.3301	10000	-2.029E-4	-2.101E-5	8249.2	8.2492E5	3.384E-3	0.5	3.0	180.012	230.19	158.7
70.34	190.5	0.3691	30.012	22.4	0.8267	6792.8198	10000	2.029E-4	2.277E-5	8491.0	8.4910E5	3.384E-3	0.5	3.0	181.012	215.79	152.4
68.34	185.4	0.3686	31.008	22.4	4.133	6917.0801	10000	1.014E-3	1.202E-4	8646.4	8.6464E5	3.383E-3	0.5	3.0	182.008	209.68	148.3
64.04	180.1	0.3555	32.000	22.4	18.19	7042.0098	10000	4.464E-3	5.605E-4	8802.5	8.8025E5	3.383E-3	0.5	3.1	183.000	196.47	144.1
60.54	172.3	0.3513	33.012	22.4	17.36	7216.6602	10000	4.261E-3	5.846E-4	9020.8	9.0208E5	3.384E-3	0.6	3.1	184.012	185.73	137.9
57.57	167.2	0.3443	34.012	22.4	10.75	7328.9102	10000	2.638E-3	3.844E-4	9161.1	9.1611E5	3.384E-3	0.6	3.1	185.012	176.63	133.8
55.14	161.9	0.3405	35.008	22.4	15.71	7441.8398	10000	3.855E-3	5.990E-4	9302.3	9.3023E5	3.384E-3	0.6	3.1	186.008	169.17	129.5
50.38	153.8	0.3275	36.012	22.4	23.97	7603.1602	10000	5.884E-3	1.013E-3	9504.0	9.5040E5	3.384E-3	0.6	3.1	187.012	154.57	123.1
47.21	148.7	0.3174	37.012	22.4	18.19	7702.8501	10000	4.464E-3	8.221E-4	9628.6	9.6286E5	3.384E-3	0.6	3.1	188.012	144.83	119.0
45.18	143.5	0.3149	38.012	22.4	23.15	7802.5801	10000	5.681E-3	1.125E-3	9753.2	9.7532E5	3.384E-3	0.6	3.2	189.012	138.60	114.8
40.41	135.3	0.2986	39.012	22.4	31.41	7945.7598	10000	7.710E-3	1.715E-3	9932.2	9.9322E5	3.384E-3	0.7	3.2	190.012	123.98	108.3
37.71	130.3	0.2895	40.008	22.4	51.25	8032.9502	10000	0.01258	3.021E-3	10041	1.0041E6	3.383E-3	0.7	3.2	191.008	115.69	104.2
36.85	125.0	0.2949	41.012	22.4	32.24	8119.9800	10000	7.913E-3	2.064E-3	10150	1.0150E6	3.384E-3	0.7	3.2	192.012	113.07	99.98
32.22	116.6	0.2763	42.012	22.4	43.81	8250.4805	10000	0.01075	3.222E-3	10313	1.0313E6	3.383E-3	0.7	3.2	193.012	98.834	93.29
29.87	111.3	0.2682	43.012	22.4	45.47	8326.3799	10000	0.01116	3.667E-3	10408	1.0408E6	3.383E-3	0.7	3.2	194.012	91.633	89.08
28.15	106.0	0.2655	44.012	22.4	44.64	8399.6299	10000	0.01096	3.970E-3	10500	1.0500E6	3.384E-3	0.7	3.3	195.012	86.363	84.83
25.45	100.5	0.2533	45.012	22.4	31.41	8474.0098	10000	7.710E-3	3.113E-3	10593	1.0593E6	3.384E-3	0.8	3.3	196.012	78.069	80.36
21.54	92.25	0.2335	46.016	22.4	50.43	8573.2197	10000	0.01238	5.926E-3	10717	1.0717E6	3.384E-3	0.8	3.3	197.016	66.090	73.80
20.10	86.89	0.2313	47.012	22.4	38.85	8636.9297	10000	9.536E-3	5.147E-3	10796	1.0796E6	3.384E-3	0.8	3.3	198.012	61.652	69.51
17.89	81.19	0.2204	48.012	22.4	54.56	8697.0098	10000	0.01339	8.277E-3	10871	1.0871E6	3.383E-3	0.8	3.3	199.012	54.892	64.95
15.63	75.39	0.2074	49.012	22.4	42.16	8752.5498	10000	0.01035	7.417E-3	10941	1.0941E6	3.384E-3	0.8	3.3	200.012	47.965	60.31
13.07	67.36	0.1940	50.016	22.4	58.69	8826.5898	10000	0.01441	0.01294	11033	1.1033E6	3.384E-3	0.8	3.4	201.016	40.099	53.89
11.14	61.45	0.1813	51.012	22.4	52.08	8875.7002	10000	0.01278	0.01379	11095	1.1095E6	3.384E-3	0.9	3.4	202.012	34.185	49.16
9.459	55.36	0.1709	52.012	22.4	51.25	8918.6104	10000	0.01258	0.01672	11148	1.1148E6	3.384E-3	0.9	3.4	203.012	29.018	44.29
8.026	49.95	0.1607	53.016	22.4	63.65	8956.1797	10000	0.01562	0.02552	11195	1.1195E6	3.383E-3	0.9	3.4	204.016	24.624	39.96
6.429	43.90	0.1465	54.012	22.4	72.75	8992.1797	10000	0.01785	0.03775	11240	1.1240E6	3.384E-3	0.9	3.4	205.012	19.724	35.12
4.934	37.57	0.1313	55.012	22.4	56.21	9022.6504	10000	0.01380	0.03981	11278	1.1278E6	3.384E-3	0.9	3.4	206.012	15.136	30.06
3.747	32.18	0.1164	56.012	22.4	82.67	9046.4404	10000	0.02029	0.07982	11308	1.1308E6	3.384E-3	0.9	3.5	207.012	11.494	25.75
2.682	25.79	0.1040	57.012	22.4	65.31	9070.4004	10000	0.01603	0.09817	11338	1.1338E6	3.384E-3	1.0	3.5	208.012	8.2279	20.63
1.987	21.99	0.09037	58.012	22.4	63.65	9081.8799	10000	0.01562	0.1317	11352	1.1352E6	3.384E-3	1.0	3.5	209.012	6.0955	17.59
0.9450	13.41	0.07047	59.012	22.4	71.92	9098.6504	10000	0.01765	0.3999	11373	1.1373E6	3.384E-3	1.0	3.5	210.012	2.8993	10.73
0.1739	5.941	0.02926	60.012	22.4	76.88	9106.1396	10000	0.01887	2.178	11383	1.1383E6	3.383E-3	1.0	3.5	211.012	0.53339	4.753

